The synthesis of pure titania and carbon-titania nano-powders in a premixed atmospheric fuel-rich flame was studied. The variation of the flame C/O ratio allows to produce both pure titania and carbon-TiO2 nanoparticles. Raman Spectroscopy, X-ray Diffraction, Atomic Force Microscopy, Electrical Low Pressure Impactor and Scanning Electron Microscopy were used to characterize the synthesized nano-powders, in terms of crystallinity, phase content, size and morphology. Produced nano-powders with a dimension of 25-40 nm are composed by both rutile and anatase phases, with rutile being the predominant one. Reactive Oxygen Species analysis performed on the synthesized nano-powders showed that the inclusion of carbon in the nano- powders results in a reduced adverse health effect, in terms of ROS production.
Carbon-Ti02 nanostructures: Flame synthesis and characterization / DE FALCO, Gianluigi; Commodo, M.; Pedata, P.; Minutolo, P.; D'Anna, Andrea. - In: MATERIALS RESEARCH SOCIETY SYMPOSIA PROCEEDINGS. - ISSN 0272-9172. - 1747:(2015), pp. 1-6. [10.1557/opl.2015.195]
Carbon-Ti02 nanostructures: Flame synthesis and characterization
DE FALCO, GIANLUIGI;D'ANNA, ANDREA
2015
Abstract
The synthesis of pure titania and carbon-titania nano-powders in a premixed atmospheric fuel-rich flame was studied. The variation of the flame C/O ratio allows to produce both pure titania and carbon-TiO2 nanoparticles. Raman Spectroscopy, X-ray Diffraction, Atomic Force Microscopy, Electrical Low Pressure Impactor and Scanning Electron Microscopy were used to characterize the synthesized nano-powders, in terms of crystallinity, phase content, size and morphology. Produced nano-powders with a dimension of 25-40 nm are composed by both rutile and anatase phases, with rutile being the predominant one. Reactive Oxygen Species analysis performed on the synthesized nano-powders showed that the inclusion of carbon in the nano- powders results in a reduced adverse health effect, in terms of ROS production.I documenti in IRIS sono protetti da copyright e tutti i diritti sono riservati, salvo diversa indicazione.